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MicroGC 3000

MicroGC 3000

Solutions for gas analysis

Specialist in "Micro-GC" applications, SRA Instruments uses AGILENT analytical modules to develop its own analyzers.

The "Micro-GC" technology was conceived to fulfill the NASA requirements. Direct heir to this design and this know-how, the AGILENT Company today proposes the Micro-GC 3000.

MicroGC 3000 (1-2 Module version)A GC 3000 may be simple (1 or 2 analysis modules) or more complete (3 or 4 modules) or portable and autonomous (1 or 2 modules, battery and gas bottle).
The Agilent GC 3000 microchromatograph is an apparatus sure, fast, precise, easy to use. Its modular design reduced the risks of breakdown while ensuring one of the most reduced downtime: each analytical module comprises an injector, a capillary column and a detector. Only a few minutes are needed to replace a module without requiring particular tool nor specific training.

 

The photograph shows a portable MicroGC3000. One distinguishes there 2 analytical modules and the carrier gas bottle.

The photograph below corresponds to a MicroGC3000 equipped with 4 analytical modules.

The Micro-GC technology offers many advantages:

  • A short run-time, typically from 20 to 180 seconds.
  • A low gas consumption and the use (quasi null) of carrier gas to actuate the valves.
  • A short implementation time (very reduced volume to be heated) associated with a great stability.
  • A nonselective detector with a very wide dynamics and an excellent reproducibility (measurement from ppm to 100 %).
  • A small overall dimensions and the portability.

The MICROGC 3000 offers higher performances even under difficult conditions (measurement of natural gas compounds with less than 0,05% RSD for retention times and less than 0,3% RSD for concentrations). The extended dynamic range of the detector allows simultaneous analysis of traces and high concentrations. The pneumatic electronic regulation allows performances to be reproducible and independent of the operator.

The photograph gives an outline of the detector or 2 injectors sizes compared to a coin of one cent euro.

Applications:

MicroGC 3000 allows measurement of most compounds from C1 to C12, of petroleum liquefied gases PLG, permanent gases (H2, O2, N2, CO, CO2, He, Ar...).

Its use relates to many activity fields:

  • Natural gas.
  • Refining, petrochemical units.
  • Gas manufactures (pure gases, calibration gases, ...).
  • Fuel cells.
  • Oil and gas prospecting.
  • Nuclear thermal power stations
  • Car industry, catalysis, ...
  • Environment (COV emission, landfill biogas, stations of treatment, hygiene, ...
  • Chemical specialities
  • Food, agrochemical industry, ...

The SRA Instruments contribution:

Reliability, simplicity, universality and dynamics, as many reasons which justify the choice of the MicroGC 3000 analytical modules.

SRA Instruments develops with lower cost general or specific applications which meet the needs for demanding users:

  • MicroTD and Mass spectrometer couplings with MicroGC 3000 (possibly on portable plate).
  • On-line explosion-proof analyzers.
  • Analyzers in 19" rack with or without PC inside.
  • Analyzers in IP66 tight box (box alone or assembled on wheels, incorporating microcomputer, microTD, mass spectrometer, gas bottles... according to needs).
  • Achievements on specifications (laboratory truck, ...)

 

Applications
 

005_Temperature programmed analysis of permanent gases
Permanent gases analysis with 1 module : argon, oxygen, nitrogen, methane and carbon monoxide in 8 minutes

021_Krypton & Xenon Analysis
Krypton and xenon at trace level in air

024_Chlorinated solvents analysis
Separation in less than 3 minutes of vinyl chloride, dichloromethane, chloroform, dichloroethane, carbon tetrachloride in air

025_Micro-GC analysis of sulfur compounds in natural gas
BTEX and sulfur compounds micro-GC separation result in natural gas with 5 different columns

026_Chlorinated hydrocarbons & BTEX
Separation of 2 different compounds families with µ-GC

029_Refinery gases analysis
Fast Analysis of light hydrocarbons and permanent gases in refinery streams in under 3 minutes is described using the new Agilent 3000 Micro Gas Chromatograph

030_Fuel cell reformer gases analysis
Rapid and accurate determination of the composition of gases produced by a catalytic reformer is important for the development and optimization of new fuel cell designs. Gas chromatography, using a micro gas chromatograph and high-resolution columns, produces a complete analysis of fuel cell gases in less than 90 seconds. Connection of the gas chromatograph directly to the output of the reactor provides valuable information for evaluating performance of new catalyst formulations and reformer designs including optimization of reformer operation

034_Formaldehyde analysis with Micro-GC
Formol detection in air

038_Detection from few ppm up to 100% with Micro-GC
The efficient linear dynamic range of Thermal Conductivity Detector is illustrated

040_Ethanol and hydrocarbons analysis
Head space sampling and microGC analysis of 5 compounds

041_Methanthiol fast analysis
Chromatogram of CH3SH analysis (< 50 seconds)

044_CO2/N2O binary mixture study
Carbon dioxyde and nitrous oxide separation at high concentration level : response linearity from 10 to 90%

045_Analysis of CO2, H2S, COS, SO2, CH3SH in Nitrogen
Carbon dioxyde, hydrogen sulfide and carbonyl sulfide analysis in nitrogen in less than 90 sec.

046_Analysis of CS2 in Air
Carbon bisulfide analysis on two different columns

047_Chloro-fluoro-carbons (CFCs) Analysis
Foranes : 143a, 142b, 141b and 365mfc separation in less than 200 seconds

048_Helium - Hydrogen separation in high concentration levels
Hydrogen quantification in a Helium matrix. Traces of oxygen and nitrogen in the same analysis.

049_Biogas type analysis (H2, N2, CH4, CO2)
Separation of 4 main compounds of biogas in less than 100 seconds as cycle time

054_Few ppm detection using the Performance-Enhanced Micro-GC
Limit of detection for Micro-GC is now lower than 1 ppm with the Performance-Enhanced TCD detector. This application note illustrates the very good sensitivity reached for few solvents

056_Near real time aromatic detection at ppb level with Micro-GC
The very high sensitivity reached with the new performance enhanced Micro-GC is shown in this application


 

SRA Instruments - Mentions légales